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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 368310Generated: October 30, 2026

Furfural → HCID 54481618, compound

https://huagongshe.com/reaction/368310

Reaction equation

Participants

RoleNameHCIDCharge
ReactantFurfuralHCID 7362—
Reactant6-(2-Imidazole-1-yl-ethoxy)-3,4-dihydro-2H-naphthalen-1-oneHCID 15486912—
SolventEthanolHCID 702—
SolventPotassium HydroxideHCID 14797—
ProductHCID 54481618HCID 5448161867.1%

Reaction Steps

According to the method of Example 6, 6-(2-imidazole-1-yl-ethoxy)-3,4-dihydro-2H-naphthalen-1-one (0.250 g, 0.98 mmol) was reacted with 2-furaldehyde (0.151 g, 1.57 mmol) in 3.0 mL of 4% KOH in EtOH for 15 hours at room temperature to afford 0.220 g (67%) of the title compound as a light tan solid, mp 109-110° C.: CI-MS m/e 334 (M+), 335 (M+ +1);

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06133303
Source datasetuspto-grants-2000_10
ORD IDord-1d1a49dee42a4636b5b0445ac554205f
Source noteuspto-grants-2000_10