HuagongsheHuagongshe Chemistry Print Report · For research reference only
Furfural → HCID 54481618, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Furfural | HCID 7362 | — |
| Reactant | 6-(2-Imidazole-1-yl-ethoxy)-3,4-dihydro-2H-naphthalen-1-one | HCID 15486912 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Potassium Hydroxide | HCID 14797 | — |
| Product | HCID 54481618 | HCID 54481618 | 67.1% |
Reaction Steps
According to the method of Example 6, 6-(2-imidazole-1-yl-ethoxy)-3,4-dihydro-2H-naphthalen-1-one (0.250 g, 0.98 mmol) was reacted with 2-furaldehyde (0.151 g, 1.57 mmol) in 3.0 mL of 4% KOH in EtOH for 15 hours at room temperature to afford 0.220 g (67%) of the title compound as a light tan solid, mp 109-110° C.: CI-MS m/e 334 (M+), 335 (M+ +1);
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06133303 |
| Source dataset | uspto-grants-2000_10 |
| ORD ID | ord-1d1a49dee42a4636b5b0445ac554205f |
| Source note | uspto-grants-2000_10 |