Benzaldehyde → HCID 178515534, compound

Participants

Reaction Steps

According to the method of Example 6, the product of Step 1 (0.271 g, 0.76 mmol) was reacted with benzaldehyde (0.121 g, 1.14 mmol) in 5 mL of 4% KOH in EtOH for 3 hours at room temperature to afford 0.125 g (46%) of the title compound as a foam which solidified on standing to give a yellow solid, mp 53-56° C.: CI-MS m/e 345 (M+ +1).

Provenance & Evidence