Hydrochloric Acid → HCID 86584173, compound

Participants

Reaction Steps

A solution of 1.0 g (3.9 mmol) of 6-[2-(1H-1-imidazolyl)ethoxy]-1,2,3,4-tetrahydro-1-naphthalenone in 10 mL of pyridine was treated with 0.41 g (5.9 mmol) of hydroxylamine×HCl and the solution heated at reflux overnight. The solution was diluted with H2O and the product collected and dried. There was obtained 0.88 g (83% yield) of the product as a white solid, mp 177-179° C. The structure was confirmed by NMR and mass spectroscopy. MS m/z 272 (M+H+).

Provenance & Evidence