Water → HCID 14271178, compound

Participants

Reaction Steps

To a solution of 1-methyl-2-benzoxypropylazide (300 mL, 1.46 mmol) in ether (10 mL), lithium aluminum hydride (167 mg, 4.38 mmol) was added. The reaction mixture was stirred at room temperature for 1 hours. Then 0.17 mL of H2O, 0.2 mL of 15% NaOH and 0.42 mL of H2O were added. The solid was filtered. The liquid was concentrated under reduced pressure to give desired product (240 mg, 92%). EI-MS m/z 180 (M+).

Provenance & Evidence