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HRID368569

反应详情

EQUATION

反应方程式

HRID 368569 的结构方程式

REACTANTS

反应物

2
结构：C[Si](C)(C)Cl
HCID6397

Chlorotrimethylsilane

C3H9ClSi

结构：CCNC(=O)c1ccccc1Cl
HCID347962

2-chloro-N-ethylbenzamide

C9H10ClNO

PRODUCTS

生成物

1
结构：CCNC(=O)c1c(Cl)cccc1[Si](C)(C)C
HCID18630379

未命名化合物

PROCEDURE

实验过程

The compound of Example f (2.2 g, 0.012 mol) was reacted with TMSCl (3.91 g, 0.036 mol) using General Method A. The title compound was recrystallized from ether/hexanes as a solid. m.p. 105-107° C.

WORKUP

后处理

  1. customThe title compound was recrystallized from ether/hexanes as a solid