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HRID368584

反应详情

EQUATION

反应方程式

HRID 368584 的结构方程式

REACTANTS

反应物

2
结构：C[Si](C)(Cl)c1ccccc1
HCID13029

Chlorodimethylphenylsilane

C8H11ClSi

结构：CCN(CC)C(=O)c1ccccc1Cl
HCID82566

2-Chloro-N,N-diethylbenzamide

C11H14ClNO

PRODUCTS

生成物

1
结构：CCN(CC)C(=O)c1c(Cl)cccc1[Si](C)(C)c1ccccc1
HCID54348567

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from the compound of Example e and 1.1 eq dimethylphenylsilyl chloride according to General Method A. Purification by HPLC with 1:9 ethyl acetate/hexanes gave 6.3 g of the desired product as a clear oil, a 91% yield.

WORKUP

后处理

  1. customPurification by HPLC with 1:9 ethyl acetate/hexanes