HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylamine → HCID 18630302, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylamine | HCID 6341 | — |
| Reactant | HCID 18630170 | HCID 18630170 | — |
| Product | HCID 18630302 | HCID 18630302 | 92% |
Reaction Steps
The compound of Example d (38.19 g, 0.13 mol) was reacted with 70% aqueous ethylamine (53 mL) according to General Method E1 and recrystallized from methylcyclohexane to afford the title compound as light tan crystals in 92% yield. m.p. 121-122° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06133252 |
| Source dataset | uspto-grants-2000_10 |
| ORD ID | ord-9f236b47024b4ca59614da048e369b60 |
| Source note | uspto-grants-2000_10 |