HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propargylamine → HCID 18630371, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propargylamine | HCID 239041 | — |
| Reactant | HCID 18630170 | HCID 18630170 | — |
| Product | HCID 18630371 | HCID 18630371 | 81% |
Reaction Steps
The compound of Example d was reacted with propargylamine (3 eq) according to General Method E1 and the crude product was recrystallized from hexanes to afford 0.55 g of the title compound as off-white needles in 81% yield. m.p. 120-121° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06133252 |
| Source dataset | uspto-grants-2000_10 |
| ORD ID | ord-447f0c18c2cf4a25bb0aa68494930042 |
| Source note | uspto-grants-2000_10 |