HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclopropylamine → HCID 18630189, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclopropylamine | HCID 69828 | — |
| Reactant | HCID 18630276 | HCID 18630276 | — |
| Product | HCID 18630189 | HCID 18630189 | 87% |
Reaction Steps
The acid chloride prepared in Example 207 was reacted with cyclopropylamine (3 eq) using General Method E1 to afford the title compound. Purification by recrystallization from hexanes gave 0.49 g of the title compound as white needles in 87% yield. m.p. 162-164° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06133252 |
| Source dataset | uspto-grants-2000_10 |
| ORD ID | ord-00b190ccd32f4203863aca5a663cc944 |
| Source note | uspto-grants-2000_10 |