HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorotrimethylsilane → 5-Chloro-N-(2-propenyl)-3-(trimethylsilyl)-2-thiophenecarboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorotrimethylsilane | HCID 6397 | — |
| Reactant | Allylamine | HCID 7853 | — |
| Reactant | 5-Chloro-2-thiophenecarboxylic acid | HCID 95048 | — |
| Product | 5-Chloro-N-(2-propenyl)-3-(trimethylsilyl)-2-thiophenecarboxamide | HCID 18630152 | — |
Reaction Steps
The title compound was prepared from 5-chloro-2-thiophenecarboxylic acid and allylamine, followed by reaction with TMSCl using the methods of Example 248 to afford 0.7 g of the title compound as a white solid. m.p. 63-66° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06133252 |
| Source dataset | uspto-grants-2000_10 |
| ORD ID | ord-5fe76d985e2d4bc7a9a5c3c2d94a96a5 |
| Source note | uspto-grants-2000_10 |