HRID368676

反应详情

EQUATION

反应方程式

HRID 368676 的结构方程式

PROCEDURE

实验过程

The compound of Example 262 (1.1 g) was reacted with 0.52 g of methyl methanethiosulfonate using procedure described for the preparation of the compound of Example 272. The title compound (0.6 g) was purified by flash chromatography with 2% ethyl acetate-hexane and recovered as a colorless oil. nD25 1.5698.

WORKUP

后处理

  1. customThe title compound (0.6 g) was purified by flash chromatography with 2% ethyl acetate-hexane
  2. customrecovered as a colorless oil