Aniline → HCID 23288695, compound

HRID 368752Notes

Reaction equation

HRID 368752 reaction equation
[O:1]1[C:5]2[CH:6]=[CH:7][C:8]([S:10]([NH:13][C:14]3[CH:15]=[C:16]([CH:20]=[C:21]([O:33][CH2:34][CH2:35][OH:36])[C:22]=3[O:23][C:24]3[CH:29]=[C:28]([O:30][CH3:31])[CH:27]=[CH:26][C:25]=3[Cl:32])[C:17](O)=[O:18])(=[O:12])=[O:11])=[CH:9][C:4]=2[O:3][CH2:2]1.[NH2:37][C:38]1[CH:43]=[CH:42][CH:41]=[CH:40][CH:39]=1>>[O:1]1[C:5]2[CH:6]=[CH:7][C:8]([S:10]([NH:13][C:14]3[CH:15]=[C:16]([CH:20]=[C:21]([O:33][CH2:34][CH2:35][OH:36])[C:22]=3[O:23][C:24]3[CH:29]=[C:28]([O:30][CH3:31])[CH:27]=[CH:26][C:25]=3[Cl:32])[C:17]([NH:37][C:38]3[CH:43]=[CH:42][CH:41]=[CH:40][CH:39]=3)=[O:18])(=[O:11])=[O:12])=[CH:9][C:4]=2[O:3][CH2:2]1

Participants

3

Reactant 2

HCID 6115AnilineHCID 17878643HCID 17878643, compound

Product 1

HCID 23288695HCID 23288695, compound

Procedure

Analogously to Example 74, by condensing 3-(benzo[1,3]-dioxol-5-sulphonylamino)-4-(2-chloro-5-methoxy-phenoxy)-5-(2-hydroxy-ethoxy)-benzoic acid with aniline there was obtained 3-(benzo[1,3]dioxol-5-sulphonylamino)-4-(2-chloro-5-methoxy-phenoxy)-5-(2-hydroxy-ethoxy)-N-phenyl-benzamide.

Sources & evidence

ORD record
ord-16ac18393feb4cafa6e0908a24fc9921
Source dataset
uspto-grants-2000_10
Patent number
US06133442

Reaction notes

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