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HRID368877

反应详情

EQUATION

反应方程式

HRID 368877 的结构方程式

REACTANTS

反应物

7
结构：C1CNCCNC1
HCID68163

1H-1,4-Diazepine, hexahydro-

C5H12N2

结构：NC(=O)c1ccc(F)cc1
HCID71572

4-Fluorobenzamide

C7H6FNO

结构：NS(=O)(=O)c1ccc(N2CCNCC2)cc1
HCID901897

4-piperazin-1-ylbenzenesulfonamide

C10H15N3O2S

结构：CNS(=O)(=O)c1ccc(F)cc1
HCID2440054

4-fluoro-N-methylbenzenesulfonamide

C7H8FNO2S

结构：OCCC1OCCc2ccccc21
HCID14141298

未命名化合物

结构：NC(=O)c1ccc(N2CCCNCC2)cc1
HCID28410931

未命名化合物

结构：CC(C(=O)N1C(=O)OC[C@@H]1Cc1ccccc1)c1ccccc1
HCID56980759

(4S)-4-(phenylmethyl)-3-(2-phenylpropionyl)-2-oxazolidinone

C19H19NO3

PRODUCTS

生成物

1
结构：CS(=O)(=O)O.NC(=O)c1ccc(N2CCCN(CC[C@@H]3OCCc4ccccc43)CC2)cc1
HCID86753847

未命名化合物

PROCEDURE

实验过程

Following the general procedure for EXAMPLE 49 and making non-critical variations (-)-2-(isochroman-1-yl)ethanol (LXXIX, 0.394 g) and 4-(homopiperazin-1-yl)benzamide (IV; 0.601 g prepared by the method of EXAMPLE 47, Step 1 from 4-fluorobenzamide, III, and homopiperazine, II) are combined to give the title compound, mp 163.75-165°; MS (m/z) 379; [α]D -41° (c, 0.975, DMF); IR (mineral oil) 1609, 1043, 1662, 1167 and 1216 cm-1.