HCID 23285404, compound → HCID 23285389, compound

HRID 369107Notes

Reaction equation

HRID 369107 reaction equation
[CH3:1][C:2]1[CH:13]=[CH:12][C:5]2[N:6]=[C:7]([CH:9]([OH:11])[CH3:10])[O:8][C:4]=2[CH:3]=1.[Cr](Cl)([O-])(=O)=O.[NH+]1C=CC=CC=1>>[C:9]([C:7]1[O:8][C:4]2[CH:3]=[C:2]([CH3:1])[CH:13]=[CH:12][C:5]=2[N:6]=1)(=[O:11])[CH3:10]

Participants

3

Reactant 2

HCID 23285404HCID 23285404, compoundHCID 178418287HCID 178418287, compound

Product 1

HCID 23285389HCID 23285389, compoundYield 20%

Procedure

6-Methyl-2-(1-hydroxyethyl)benzoxazole as the starting material was reacted with pyridinium chlorochromate in the same manner as in Reference Example 1 (4) iii) to obtain 2-acetyl-6-methylbenzoxazole (yield, 20%).

Sources & evidence

ORD record
ord-dcfe5781348e46d2a3de216efdd4b479
Source dataset
uspto-grants-2000_10
Patent number
US06136831

Reaction notes

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