HCID 23285598, compound → HCID 23285629, compound

HRID 369198Notes

Reaction equation

HRID 369198 reaction equation
[I-].[Cl:2][C:3]1[C:4]([CH2:12][CH:13]([C:19]([O:21][CH3:22])=[O:20])[CH2:14][N+](C)(C)C)=[CH:5][C:6]2[O:10][CH2:9][O:8][C:7]=2[CH:11]=1>O>[Cl:2][C:3]1[C:4]([CH2:12][C:13](=[CH2:14])[C:19]([O:21][CH3:22])=[O:20])=[CH:5][C:6]2[O:10][CH2:9][O:8][C:7]=2[CH:11]=1

Participants

3

Reactant 1

HCID 23285598HCID 23285598, compound

Product 1

HCID 23285629HCID 23285629, compoundYield 87.4%

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

The operation is carried out as in Stage 3 of Example 1 starting with 484 mg of the product obtained in Stage 3 above, 5 ml of water and 2 ml of 2N soda. In this way 244 mg of expected product (white powder) is obtained.

Sources & evidence

ORD record
ord-d2fc5a3f3d3b4f31b25916488d9161ff
Source dataset
uspto-grants-2000_10
Patent number
US06136842

Reaction notes

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