HCID 23285629, compound → HCID 23285632, compound

HRID 369199Notes

Reaction equation

HRID 369199 reaction equation
[Cl:1][C:2]1[C:3]([CH2:11][C:12](=[CH2:17])[C:13]([O:15]C)=[O:14])=[CH:4][C:5]2[O:9][CH2:8][O:7][C:6]=2[CH:10]=1.[C:18]([OH:21])(=[S:20])[CH3:19]>>[C:18]([S:20][CH2:17][CH:12]([CH2:11][C:3]1[C:2]([Cl:1])=[CH:10][C:6]2[O:7][CH2:8][O:9][C:5]=2[CH:4]=1)[C:13]([OH:15])=[O:14])(=[O:21])[CH3:19]

Participants

3

Reactant 2

HCID 23285629HCID 23285629, compoundHCID 178418634HCID 178418634, compound

Product 1

HCID 23285632HCID 23285632, compound

Procedure

The operation is carried out as in Stage 4 of Example 1 starting with 223 mg of product obtained in Stage 4 above and 0.16 ml thioacetic acid. In this way 172 mg of expected product is obtained.

Sources & evidence

ORD record
ord-739ecd136c3248aba1287131af89fd86
Source dataset
uspto-grants-2000_10
Patent number
US06136842

Reaction notes

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