Diethyl Ether → HCID 22467203, compound

HRID 369344Notes

Reaction equation

HRID 369344 reaction equation
[Br:1][C:2]1[CH:10]=[C:9]2[C:5]([C:6]([CH:12]([C:26]3[C:34]([Cl:35])=[CH:33][C:29]4[O:30][CH2:31][O:32][C:28]=4[CH:27]=3)[C:13](NS(C3C=CC(C)=CC=3)(=O)=O)=[O:14])=[CH:7][N:8]2C)=[CH:4][CH:3]=1.[CH2:36]([O:38]CC)C>CCCCCC>[Br:1][C:2]1[CH:10]=[C:9]2[C:5]([C:6]([CH:12]([C:26]3[C:34]([Cl:35])=[CH:33][C:29]4[O:30][CH2:31][O:32][C:28]=4[CH:27]=3)[C:13]([O:38][CH3:36])=[O:14])=[CH:7][NH:8]2)=[CH:4][CH:3]=1

Participants

4

Reactant 2

HCID 3283Diethyl EtherHCID 22467220HCID 22467220, compound

Product 1

HCID 22467203HCID 22467203, compound

Reagents, catalysts & solvents 1

HCID 8058HexaneSolvent

Procedure

The subtitle compound was prepared following the procedure of Example 92(c), using methyl 2-bromo-2-(6-chloro-1,3-benzodioxol-5-yl)acetate from step (b), m.p. 172-174° C. from diethyl ether and hexane.

Sources & evidence

ORD record
ord-242a23a65c6a421b9459425a47b530b9
Source dataset
uspto-grants-2000_10
Patent number
US06136843

Reaction notes

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