HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphoric Acid → 3,4-Dimethylpyrazolium dihydrogen phosphate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphoric Acid | HCID 1004 | — |
| Reactant | HCID 178430906 | HCID 178430906 | — |
| Solvent | Water | HCID 962 | — |
| Product | 3,4-Dimethylpyrazolium dihydrogen phosphate | HCID 71435873 | 98% |
Reaction Steps
96 g (1.0 mol) of 3,4-dimethylpyrazole were dissolved in 115 g (1.0 mol) of phosphoric acid (85%) at room temperature. The water contained in the phosphoric acid was evaporated. After a few hours, the title compound crystallized out from the oil initially present (yield 98%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06139596 |
| Source dataset | uspto-grants-2000_10 |
| ORD ID | ord-ca28189163594ff7aeb04962f28ada04 |
| Source note | uspto-grants-2000_10 |