HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus tribromide → HCID 18352496, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus tribromide | HCID 24614 | — |
| Reactant | HCID 11041251 | HCID 11041251 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 18352496 | HCID 18352496 | 93% |
Reaction Steps
According to example 17, 5.47 g of 2-cyclopentylbenzyl alcohol was treated with 1.03 mL of PBr3 in 25 mL of anhydrous CH2Cl2 to afford 6.9 g (93%) of 2-cyclopentylbenzyl bromide as a clear liquid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06140100 |
| Source dataset | uspto-grants-2000_10 |
| ORD ID | ord-2500025ce2b94777a7de4986695f87e9 |
| Source note | uspto-grants-2000_10 |