HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus tribromide → 3-Cyclopentylbenzyl bromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus tribromide | HCID 24614 | — |
| Reactant | 3-Cyclopentylbenzyl alcohol | HCID 53788593 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 3-Cyclopentylbenzyl bromide | HCID 18352477 | 100% |
Reaction Steps
According to example 17, 5.77 g of 3-cyclopentylbenzyl alcohol was treated with 1.09 mL of PBr3 in 25 mL of anhydrous CH2Cl2 to afford 7.85 g (100%) of 3-cyclopentylbenzyl bromide as a light yellow liquid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06140100 |
| Source dataset | uspto-grants-2000_10 |
| ORD ID | ord-ef58c595a3c144afa4f084fa3c0a633c |
| Source note | uspto-grants-2000_10 |