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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 370455Generated: October 30, 2026

Methyl isothiocyanate → HCID 13131636, compound

https://huagongshe.com/reaction/370455

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethyl isothiocyanateHCID 11167—
ReactantHCID 13131604HCID 13131604—
Solvent1,2-DimethoxyethaneHCID 8071—
ProductHCID 13131636HCID 1313163661.2%

Reaction Steps

3.7 g (0.05M) of methyl isothiocyanate in 10 ml of dimethoxyethane is dripped into 8.0 g (0.05M) of 2-amino-4,7-dimethylisoindoline in 50 ml of 1,2-dimethoxyethane. Conventional processing was conducted after 15 hours, yielding 7.1 g of 1-methyl-3-(4,7-dimethylisoindolin-2-yl)-thiourea.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04526897
Source datasetuspto-grants-1985_07
ORD IDord-198a4f743bc748ca991dbc7d17ba0910
Source noteuspto-grants-1985_07