Morpholine → HCID 13912220, compound

HRID 370474Notes

Reaction equation

HRID 370474 reaction equation
Br[CH2:2][C:3]1[CH:4]=[CH:5][C:6]2[O:10][C:9]([N+:11]([O-:13])=[O:12])=[C:8]([C:14]3[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=3)[C:7]=2[CH:20]=1.[NH:21]1[CH2:26][CH2:25][O:24][CH2:23][CH2:22]1>C(O)C>[N+:11]([C:9]1[O:10][C:6]2[CH:5]=[CH:4][C:3]([CH2:2][N:21]3[CH2:26][CH2:25][O:24][CH2:23][CH2:22]3)=[CH:20][C:7]=2[C:8]=1[C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1)([O-:13])=[O:12]

Participants

4

Reactant 2

HCID 8083MorpholineHCID 13531604HCID 13531604, compound

Product 1

HCID 13912220HCID 13912220, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

Using the method of Example 1, 5-bromomethyl-2-nitro-3-phenylbenzofuran is reacted with morpholine in ethanol to provide yellow crystals of N-(2-nitro-3-phenyl-5-benzofuranylmethyl)-morpholine, m.p. 151°-154° C., having the structure ##STR13##

Sources & evidence

ORD record
ord-8f44bfbb3dbc4d80a264cdcb2e4bf6ce
Source dataset
uspto-grants-1985_07
Patent number
US04526896

Reaction notes

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