HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic acid, azido-, ethyl ester → HCID 13518828, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic acid, azido-, ethyl ester | HCID 69480 | — |
| Reactant | p-Toluenesulphonyl cyanide | HCID 87946 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 13518828 | HCID 13518828 | — |
Reaction Steps
A mixture of 7.24 g. of p-toluenesulfonyl cyanide and 5.16 g. of ethyl azidoacetate (Dictionary of Organic Compounds, Vol. 1, p. 307) in 150 ml. of benzene is heated at reflux for 12 hours. The residue after evaporation is recrystallized from benzene-hexane, m.p. 98°-100° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04526978 |
| Source dataset | uspto-grants-1985_07 |
| ORD ID | ord-4622c24bbf434f6d86298449c505efe1 |
| Source note | uspto-grants-1985_07 |