2-Nitrobenzoyl chloride → HCID 178522658, compound

Participants

Reaction Steps

To a solution of 10.3 g of 5-aminotetrazole monohydrate in 300 ml of tetahydrofuran and 15 ml of water was added 9.3 g of 2-nitrobenzoyl chloride. The solution was allowed to stand for 30 minutes before it was diluted with 200 ml of water and stored in a refrigerator for 72 hours. The solid which formed was separated by filtration to give 2-nitro-N-(1H-tetrazol-5-yl)-benzamide melting at about 272°-273° C. with decomposition.

Provenance & Evidence