HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 178478602, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 3-Amino-4-[3-(4-piperidinomethyl-2-pyridyloxy)propylamino]-1,2,5-thiadiazole 1-oxide | HCID 15961341 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178478602 | HCID 178478602 | — |
Reaction Steps
The product of Step B (5.0 g; 13.7 mmoles) was dissolved in 80 ml of methanol and treated with 9.1 ml of concentrated HCl. After stirring at ambient temperature for 4.5 hours, the solution was evaporated to dryness under reduced pressure to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04528377 |
| Source dataset | uspto-grants-1985_07 |
| ORD ID | ord-c524f7253f9f42119bb7765c9b6f9742 |
| Source note | uspto-grants-1985_07 |