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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 370911Generated: October 26, 2026

N-Methylbenzamide → N-Methylbenzimidoyl chloride

https://huagongshe.com/reaction/370911

Reaction equation

Participants

RoleNameHCIDCharge
ReactantN-MethylbenzamideHCID 11954—
ReactantThionyl ChlorideHCID 24386—
ProductN-Methylbenzimidoyl chlorideHCID 57627791%

Reaction Steps

N-Methyl benzamide (55.97 g., 418 mmole) and thionyl chloride (114.7 g, 0.96 mole) were treated as in Example I. Yield 58.4 g (91%) of the title compound, b.p. 80°-90° C. (~0.1 mm Hg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04528382
Source datasetuspto-grants-1985_07
ORD IDord-a8c72cef2c564185b95a22d00e3d16a7
Source noteuspto-grants-1985_07