HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → N-Methyl 4-Chlorobenzimidoyl Chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | Benzamide, 4-chloro-N-methyl- | HCID 101339 | — |
| Product | N-Methyl 4-Chlorobenzimidoyl Chloride | HCID 12341506 | 83.4% |
Reaction Steps
N-Methyl 4-chlorobenzamide (42.6 g, 251 mmole) and thionyl chloride (153.3 g, 1.28 mole) were reacted as in Example I to yield 39.3 g (83.4%) of the title compound, b.p. 125° C. (15 mm Hg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04528382 |
| Source dataset | uspto-grants-1985_07 |
| ORD ID | ord-aa49b43da37c4071bcf1eef74fe1037b |
| Source note | uspto-grants-1985_07 |