HuagongsheHuagongshe Chemistry Print Report · For research reference only
Perchloric Acid → HCID 20275539, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Perchloric Acid | HCID 24247 | — |
| Reactant | Chlorosulfonic acid | HCID 24638 | — |
| Reactant | N-Methyl 4-Chlorobenzimidoyl Chloride | HCID 12341506 | — |
| Reactant | Methyl 1,4-dimethyl-1H-pyrrole-2-acetate | HCID 13221886 | — |
| Product | HCID 20275539 | HCID 20275539 | — |
Reaction Steps
The title compound was prepared as in Example X from N-methyl 4-chlorobenzimidoyl chloride (6.07 g, 32.3 mmole), chlorosulfonic acid (0.46 g, 4.0 mmole), methyl 1,4-dimethyl-1H-pyrrole-2-acetate (6.64 g, 39.8 mmole), and 70% perchloric acid (5.5 g, 38.3 mmole) to yield 9.3 g (69%) of a bright yellow solid, m.p. 168°-171° C. (dec).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04528382 |
| Source dataset | uspto-grants-1985_07 |
| ORD ID | ord-929fba54c36c4c178606aad5ca27ae1d |
| Source note | uspto-grants-1985_07 |