Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Perchloric Acid → Methyl 1-Methyl-5[(methylimino)(4-methylphenyl)methyl]-1H-pyrrole-2-acetate Perchlorate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Perchloric Acid | HCID 24247 | — |
| 반응물 | Chlorosulfonic acid | HCID 24638 | — |
| 반응물 | Methyl 1-methylpyrrol-2-acetate | HCID 103992 | — |
| 반응물 | N-Methyl 4-Methylbenzimidoyl Chloride | HCID 12410496 | — |
| 생성물 | Methyl 1-Methyl-5[(methylimino)(4-methylphenyl)methyl]-1H-pyrrole-2-acetate Perchlorate | HCID 18598661 | — |
반응 단계
The title compound was prepared as in Example X from N-methyl 4-methylbenzimidoyl chloride (5.9 g, 35 mmole), chlorosulfonic acid (0.41 g, 3.5 mmole), methyl 1-methyl-1H-pyrrole-2-acetate (5.4 g, 35 mmole), and 70% perchloric acid (5.5 g, 38.5 mmole) to yield 4.0 g (30%) of a green solid, m.p. 155°-159° C. (dec).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04528382 |
| 출처 데이터셋 | uspto-grants-1985_07 |
| ORD ID | ord-e23d796ecec24cf48188e4fb4c036830 |
| 출처 메모 | uspto-grants-1985_07 |