HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13519565, compound → HCID 13519557, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13519565 | HCID 13519565 | — |
| Catalyst | Hydrochloric Acid | HCID 313 | — |
| Catalyst | Platinum oxide (PtO) | HCID 82844 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 13519557 | HCID 13519557 | 91.9% |
Reaction Steps
A mixture of 8.0 g of the above dicarboximide, 0.8 g of platinum oxide and 3 drops of concentrated hydrochloric acid in 150 ml of ethyl acetate was hydrogenated in a Parr apparatus. The reaction mixture was filtered and the filtrate was concentrated in vacuo giving 7.4 g of 3a-(3,4-dichlorophenyl)hexahydro-2-methyl-4,7-ethano-1H-isoindole-1,3(2H)-dione as straw colored crystals, mp 126°-134° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04529736 |
| Source dataset | uspto-grants-1985_07 |
| ORD ID | ord-bc7608f50fa848c4a7ee72cc8488dc4e |
| Source note | uspto-grants-1985_07 |