HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propionic anhydride → HCID 70491093, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propionic anhydride | HCID 31263 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Reactant | HCID 54515114 | HCID 54515114 | — |
| Product | HCID 70491093 | HCID 70491093 | — |
Reaction Steps
Acylation of 2-[4-(5-phenyl-2-pentyloxy)-2-benzyloxyphenyl]-4-piperidinol with propionic anhydride by the method of Example 8, followed by lithium aluminum hydride reduction of the resulting N,O-dipropionyl intermediate by the method of Example 9, Part A, and finally, debenzylation by the method of Example 9, Part B, provides the title compound in like manner.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04529732 |
| Source dataset | uspto-grants-1985_07 |
| ORD ID | ord-ff32dff8408a4797a67663bba44c5199 |
| Source note | uspto-grants-1985_07 |