Diisopropylamine → HCID 54334711, compound

Participants

Reaction Steps

A solution of diisopropylamine (72 mL, 0.512 mole) in 75 mL of anhydrous ether was added dropwise to a cold (ice bath) solution of 106 mL (1.02 moles) of thiophosphoryl chloride in 300 mL of anhydrous ether under an argon atmosphere. The resultant slurry was allowed to slowly warm to room temperature. After filtering to remove isopropylamine hydrochloride, the filtrate was concentrated under vacuum to provide a red oil (45.2 g, 75.4%).

Provenance & Evidence