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HRID371322

反应详情

EQUATION

反应方程式

HRID 371322 的结构方程式

REACTANTS

反应物

2
结构：Cc1cccc2c1NC(=O)C2=O
HCID14313

7-Methylisatin

C9H7NO2

结构：BrBr
HCID24408

Bromine

Br2

PRODUCTS

生成物

1
结构：O=C1Nc2c(CBr)cccc2C1=O
HCID13519800

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(Cl)Cl
溶剂HCID6365

1,1-Dichloroethane

C2H4Cl2

PROCEDURE

实验过程

The 7-methylisatin (16.1 g, 0.1 mole) is suspended in dichloroethane (2000 ml) and the suspension is heated and irradiated with a high intensity light source to the reflux point. Bromine (24.3 g, 0.15 mole) is added dropwise over a one hour period.

WORKUP

后处理

  1. temperaturethe suspension is heated
  2. customirradiated with a high intensity light source to the reflux point