HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53818886, compound → HCID 13519803, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53818886 | HCID 53818886 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 13519803 | HCID 13519803 | — |
Reaction Steps
A solution of 2-nitro-1,3-benzenediacrylic acid diethyl ester (3.5 g, 0.011 mole) in absolute ethanol (100 ml) is treated with hydrogen at 1 atmosphere pressure for 12 hours in the presence of 20% Pd/C. The mixture is filtered and concentrated at reduced pressure to yield 1,2,3,4-tetrahydro-2-oxo-8-quinolinepropanoic acid ethyl ester, mp 102°-103° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04530929 |
| Source dataset | uspto-grants-1985_07 |
| ORD ID | ord-482ba82030834efaa2ec10e3b0158c05 |
| Source note | uspto-grants-1985_07 |