HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methacryloyl chloride → (4-Nitrophenyl)methyl 2-methylprop-2-enoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methacryloyl chloride | HCID 13528 | — |
| Reactant | 4-Nitrobenzyl alcohol | HCID 69275 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | (4-Nitrophenyl)methyl 2-methylprop-2-enoate | HCID 20188873 | 64.6% |
Reaction Steps
From the reaction of 52.3 g (0.5 m) methacryloyl chloride and 76.6 g (0.5 m) of p-nitrobenzyl alcohol and 50.6 g triethylamine was isolated 71.5 g (34.5%) of p-nitrobenzyl methacrylate as pale-yellow crystals, mp--87°-88° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04532269 |
| Source dataset | uspto-grants-1985_07 |
| ORD ID | ord-afe7a6e6d538416d8aa5db7d4ab07e6c |
| Source note | uspto-grants-1985_07 |