HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Azido-N-[4-[(4-fluorophenyl)sulfonyl]phenyl]acetamide → HCID 20273397, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Azido-N-[4-[(4-fluorophenyl)sulfonyl]phenyl]acetamide | HCID 20273408 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 20273397 | HCID 20273397 | — |
Reaction Steps
A 2.0 g portion of this azide was dissolved in 40 ml of p-dioxane and subjected to hydrogenation with Raney nickel catalyst for 1.5 hours. The mixture was filtered, the filtrate concentrated to a residue and recrystallized from ethanol giving 944 mg of the desired product as white crystals, mp 181°-184° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04532349 |
| Source dataset | uspto-grants-1985_07 |
| ORD ID | ord-15aa7ed2494c42739c8f06bad45b8a00 |
| Source note | uspto-grants-1985_07 |