HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 371520Generated: October 26, 2026
2-Chloro-6-methylphenol → 2-Chloro-4-[(3,4-dichlorophenyl)methyl]-6-methylphenol
https://huagongshe.com/reaction/371520
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 2-Chloro-6-methylphenol | HCID 6898 | — |
| Reactant | 3,4-Dichlorobenzyl chloride | HCID 7609 | — |
| Solvent | Water | HCID 962 | — |
| Product | 2-Chloro-4-[(3,4-dichlorophenyl)methyl]-6-methylphenol | HCID 20273489 | — |
Reaction Steps
90.4 g (0.63 mol) 2-chloro-6-methylphenol are brought to reaction with 149.4 g (0.765 mol) 3,4-dichlorobenzylchloride and 2.4 g water-free, finely mortared ZnCL2 without solvent. After stirring 5-6 h at 60° C. the reaction mixture is subsequently worked up by washing three times, each with 100 ml water.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04532367 |
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| Source dataset | uspto-grants-1985_07 |
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| ORD ID | ord-3b7da3a114114c5ab5eb9a01eb9ae00a |
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| Source note | uspto-grants-1985_07 |
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