HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → 2-Chloro-4-[(4-chlorophenyl)methyl]-6-methylphenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 2-Chloro-6-methylphenol | HCID 6898 | — |
| Reactant | 1-Chloro-4-(chloromethyl)benzene | HCID 7723 | — |
| Catalyst | Zincchloride | HCID 3007855 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | 2-Chloro-4-[(4-chlorophenyl)methyl]-6-methylphenol | HCID 23319416 | — |
Reaction Steps
178.1 g (1.25 mol) 2-chloro-6-methylphenol and 80.5 g (0.5 mol) 4-chlorobenzyl chloride are dissolved in 300 ml dry chloroform. 40 g water-free, finely mortared ZnCl2 are subsequentlyadded.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04532367 |
| Source dataset | uspto-grants-1985_07 |
| ORD ID | ord-b42a7c7a56254d26ad242311a2889111 |
| Source note | uspto-grants-1985_07 |