HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formamide → HCID 20355973, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formamide | HCID 713 | — |
| Reactant | 2,2,3-Trichloropropionaldehyde | HCID 24623 | — |
| Product | HCID 20355973 | HCID 20355973 | 82.4% |
Reaction Steps
A mixture consisting of 16.2 gm of 2,2,3-trichloropropionaldehyde and 4.5 gm of formamide was stirred on a boiling water bath for 30 minutes. Recrystallization of the reaction product from benzene yielded 17 gm of the desired compound, m.p. 105°-109° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04087533 |
| Source dataset | uspto-grants-1978_05 |
| ORD ID | ord-0113a598cc1e40a8a4cd9f6f5dd92412 |
| Source note | uspto-grants-1978_05 |