Aniline → 6-Hydroxy-2-anilinocarbonyl-2,3-dihydro-1,4-benzodioxin

HRID 37173Notes

Reaction equation

HRID 37173 reaction equation
[NH2:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[OH:8][C:9]1[CH:21]=[CH:20][C:12]2[O:13][CH:14]([C:17](O)=[O:18])[CH2:15][O:16][C:11]=2[CH:10]=1>>[OH:8][C:9]1[CH:21]=[CH:20][C:12]2[O:13][CH:14]([C:17]([NH:1][C:2]3[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=3)=[O:18])[CH2:15][O:16][C:11]=2[CH:10]=1

Participants

3

Reactant 2

HCID 6115AnilineHCID 108780626-Hydroxy-2,3-dihydro-1,4-benzodioxin-2-carboxylic acid

Product 1

HCID 118077896-Hydroxy-2-anilinocarbonyl-2,3-dihydro-1,4-benzodioxinYield 75%

Procedure

That compound is obtained in a yield of 75% starting frown aniline and 6-hydroxy-2,3-dihydro -1,4-benzodioxin-2-carboxylic acid.

Workup

  1. customThat compound is obtained in a yield of 75%

Sources & evidence

ORD record
ord-592ff11bd03f4b75afea813adfce1902
Source dataset
uspto-grants-1995_05
Patent number
US05420132

Reaction notes

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