Aniline → 7-Hydroxy-2-anilinocarbonyl-1,4-benzodioxin

HRID 37174Notes

Reaction equation

HRID 37174 reaction equation
[NH2:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[OH:8][C:9]1[CH:10]=[CH:11][C:12]2[O:17][CH:16]=[C:15]([C:18](O)=[O:19])[O:14][C:13]=2[CH:21]=1>>[OH:8][C:9]1[CH:10]=[CH:11][C:12]2[O:17][CH:16]=[C:15]([C:18]([NH:1][C:2]3[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=3)=[O:19])[O:14][C:13]=2[CH:21]=1

Participants

3

Reactant 2

HCID 6115AnilineHCID 109323117-Hydroxy-1,4-benzodioxin-2-carboxylic acid

Product 1

HCID 109016387-Hydroxy-2-anilinocarbonyl-1,4-benzodioxinYield 63%

Procedure

That compound is obtained in a yield of 63% starting from aniline and 7-hydroxy-1,4-benzodioxin-2-carboxylic acid.

Workup

  1. customThat compound is obtained in a yield of 63%

Sources & evidence

ORD record
ord-97cbbf2420ad4763ad9f0c4aac9a7c01
Source dataset
uspto-grants-1995_05
Patent number
US05420132

Reaction notes

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