Allyl bromide → HCID 20356329, compound

Participants

Reaction Steps

A solution of 10-bornanamine (obtained by basification, with sodium hydroxide, of 1.517g. 10-bornanamine hydrochloride) in acetone (20ml) containing allyl bromide (0.68ml) was kept at room temperature for 3.5 days during which time a small amount of solid crystallized. The solution was evaporated to about one third of its original volume, cooled to 0° and the crystalline material collected by filtration to give title compound m.p. above 295° with slow decomp. (Found: C,56.6; H,8.6; N,5.1. C13H24BrN requires C,56.95; H,8.8; N,5.1%).

Provenance & Evidence