HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 37187Generated: October 29, 2026
Dimethylformamide → HCID 19934803, compound
https://huagongshe.com/reaction/37187
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 3-Bromo-N-trityl-1-propanamine | HCID 256581 | — |
| Reactant | [2-(2-Methoxyphenoxy)ethyl](methyl)amine hydrochloride | HCID 19749083 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 19934803 | HCID 19934803 | — |
Reaction Steps
8.05 g (0.0370 mol) of N-methyl-2-(2-methoxyphenoxy) ethylamine hydrochloride, 15.5 g (0. 0407 mol) of N-triphenylmethyl-3-bromopropylamine, (0.0925 mol) of potassium carbonate and 75 ml of N,N-dimethylformamide are introduced, under argon, into a 500 ml, three-necked, round-bottomed flask. The mixture is stirred for 15.5 h at 90° C. The reaction mixture is treated with a mixture of water and ice and extracted with ethyl acetate. The organic phase is washed with water, dried over sodium sulphate and concentrated under reduced pressure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05420130 |
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| Source dataset | uspto-grants-1995_05 |
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| ORD ID | ord-39883375f053417189b803f1e6ae0faf |
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| Source note | uspto-grants-1995_05 |
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