HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Ethyl cyclohexylamine → 2-Amino-N-cyclohexyl-N-ethyl-5-methoxy-benzylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Ethyl cyclohexylamine | HCID 21609 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | (2-Amino-5-methoxyphenyl)methanol | HCID 13756678 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 2-Amino-N-cyclohexyl-N-ethyl-5-methoxy-benzylamine | HCID 20319198 | — |
Reaction Steps
2-Amino-N-cyclohexyl-N-ethyl-5-methoxy-benzylamine was prepared from 2-amino-5-methoxy-benzyl alcohol, thionyl chlorie and N-ethyl-cyclohexylamine analogous to Example 1. Proof of structure by IR- and UV-spectra. IR-spectrum (methylenechloride): 3250 cm-1NH2 ; 3400 cm-1NH2 ; 2830 cm-1OCH3 ; 2800 cm-1N-ethyl (shoulder); 2850 cm-1 aliphatic hydrocarbon; 2930 cm-1 aliphatic hydrocarbon; 1500 cm-1C=C; 1600 cm-1C=C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | USRE029628 |
| Source dataset | uspto-grants-1978_05 |
| ORD ID | ord-2cde5289b1b2412795d4a76dc6a93da3 |
| Source note | uspto-grants-1978_05 |