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Hydrochloric Acid → 2-[4-(2-Methoxyphenyl)piperazin-1-yl]ethanamine trihydrochloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | 2-[4-(2-Methoxyphenyl)piperazin-1-yl]-N-(triphenylmethyl)ethanamine | HCID 15718288 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | 2-[4-(2-Methoxyphenyl)piperazin-1-yl]ethanamine trihydrochloride | HCID 19934808 | — |
反応手順
9.24 g of 2-[4-(2-methoxyphenyl)piperazin-1-yl)-N-(triphenylmethyl)ethanamine are dissolved in 400 ml of methanol and, after homogenization, a stream of gaseous hydrochloric acid is passed into the solution for 10 min. The precipitate is collected, rinsed with methanol and dried under vacuum. 5.33 g of white solid are obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05420130 |
| 出典データセット | uspto-grants-1995_05 |
| ORD ID | ord-0f7caca2e5c54b8b9c8794e8848e7290 |
| 出典メモ | uspto-grants-1995_05 |