Sodium Carbonate → HCID 20352260, compound

HRID 371942Notes

Reaction equation

HRID 371942 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]23[CH2:13][CH:12]2[CH2:11][NH:10][CH2:9]3)=[CH:4][CH:3]=1.C(=O)([O-])[O-].[Na+].[Na+].[O:20]1[CH:24]=[CH:23][CH:22]=[C:21]1[C:25](Cl)=[O:26]>>[O:20]1[CH:24]=[CH:23][CH:22]=[C:21]1[C:25]([N:10]1[CH2:11][CH:12]2[C:8]([C:5]3[CH:4]=[CH:3][C:2]([Cl:1])=[CH:7][CH:6]=3)([CH2:13]2)[CH2:9]1)=[O:26]

Participants

4

Reactant 3

HCID 10340Sodium CarbonateHCID 682422-Furancarbonyl chlorideHCID 101303311-(4-Chlorophenyl)-3-azabicyclo[3.1.0]hexane

Product 1

HCID 20352260HCID 20352260, compound

Procedure

Following the procedure of Example 8, 19.35 g. of 1-p-chlorophenyl-3-azabicyclo[3.1.0]hexane, 10.59 g. of sodium carbonate and 13.05 g. of 2-furoyl chloride are reacted to produce the product as a dark brown gum.

Sources & evidence

ORD record
ord-ad85289512864b2d8a2f3810cfca1c0b
Source dataset
uspto-grants-1978_05
Patent number
US04088652

Reaction notes

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