HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → 3-Acetyl-1-(p-acetamidophenyl)-3-azabicyclo[3.1.0]hexane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | 3-Acetyl-1-(p-aminophenyl)-3-azabicyclo[3.1.0]hexane | HCID 20468332 | — |
| Solvent | Sodium Diacetate | HCID 23662384 | — |
| Product | 3-Acetyl-1-(p-acetamidophenyl)-3-azabicyclo[3.1.0]hexane | HCID 20352249 | — |
Reaction Steps
A solution of 3-acetyl-1-(p-aminophenyl)-3-azabicyclo[3.1.0]hexane in aqueous acetic acid-sodium acetate is treated with acetic anhydride at ambient temperature. The reaction mixture is chilled and filtered to give 3-acetyl-1-(p-acetamidophenyl)-3-azabicyclo[3.1.0]hexane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04088652 |
| Source dataset | uspto-grants-1978_05 |
| ORD ID | ord-f94df4f344024768bd329a144a2703ea |
| Source note | uspto-grants-1978_05 |