HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Potassium Carbonate → (4-Bromophenyl)(2-butylpyrazolo(1,5-a)pyridin-3-yl) methanone
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Potassium Carbonate | HCID 11430 | — |
| Edukt | 1-Aminopyridin-1-ium 2,4,6-trimethylbenzene-1-sulfonate | HCID 13028200 | — |
| Edukt | 1-(4-Bromophenyl) 2-heptyn-1-one | HCID 54449136 | — |
| Lösungsmittel | Acetonitrile | HCID 6342 | — |
| Produkt | (4-Bromophenyl)(2-butylpyrazolo(1,5-a)pyridin-3-yl) methanone | HCID 21472334 | — |
Reaktionsschritte
A mixture of 2.5 g of N-aminopyridinium mesitylene sulfonate (prepared by Synthesis, 1977 page 1, TAMURA, et al.), 25 ml of acetonitrile and 3.5 g of potassium carbonate was stirred for 15 minutes at ambient temperature and then the 2.27 g of the product of Step A in solution in 25 ml of acetonitrile were added.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05420138 |
| Quelldatensatz | uspto-grants-1995_05 |
| ORD ID | ord-87177dc4843a45a081558e110fdea74d |
| Quellennotiz | uspto-grants-1995_05 |