HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → 4-[(2-Butyl pyrazolo(1,5-a) pyridin-3-yl) carbonyl]benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | (2-Butylpyrazolo(1,5-a)pyridin-3-yl)carbonyl benzonitrile | HCID 86748690 | — |
| Solvent | Water | HCID 962 | — |
| Product | 4-[(2-Butyl pyrazolo(1,5-a) pyridin-3-yl) carbonyl]benzoic acid | HCID 21472332 | — |
Reaction Steps
A mixture of 845 mg of the product of Example 2 and 15 ml of a mixture in equal proportions of sulfuric acid, acetic acid and water was refluxed for 2 hours and the mixture was cooled down, taken up in water, filtered, washed with water and dried at 80° C. under reduced pressure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05420138 |
| Source dataset | uspto-grants-1995_05 |
| ORD ID | ord-61b16523a7764a7a8d917dd5cae5cf31 |
| Source note | uspto-grants-1995_05 |