HCID 20353242, compound → HCID 20353225, compound

Participants

Reaction Steps

A solution of 5.0 g of 5,11-dinitro-2-cyclopentylmethyl-2,3,8,12b-tetrahydro-1H-3a,8-methanodibenzo[3,4:6,7]cyclohepta[1,2-c]pyrrole in tetrahydrofuran was hydrogenated at 50 lbs. pressure and room temperature with 0.2 g of platinum oxide catalyst to give 5.3 g of 5,11 -diamino-2-cyclopentylmethyl-2,3,8,12b-tetrahydro-1H-3a,8-methanodibenzo[3,4:6,7]cyclohepta[1,2-c]pyrrole as an oil; nmr spectrum: δ 1.0-4.0 (m, 19); 3.4 (s, 4); 6.2-6.7 (m, 4); 6.8-7.0 (m, 2).

Provenance & Evidence